Now showing items 1-5 of 26

    • Imine-tetrahydroquinazoline tautomerism in a tosilated Schiff base 

      García Deibe, Ana María; Portela García, Cristina; Sanmartín Matalobos, Jesús; Fondo Busto, María Matilde (MDPI, 2010)
      Condensation of the selectively tosilated N-(2-aminobenzyl)-4-methylbenzenesulfonamide with 2-hydroxybenzaldehyde gives rise to (E)-N-(2-(2- hydroxybenzylideneamino)benzyl)-4-methylbenzenesulfonamide in the solid state, ...
    • Synthesis of dicompartimental schiff base ligands : Crystal structure of (n-n'-bis(3- methoxy or 3-ethoxysalicylidene)-1,2-diamine-2-methylpropane 

      Vázquez Fernández, María de los Ángeles; Fernández García, María Isabel; Fernández Fernández, Beatriz; González Noya, Ana María; Rodríguez Doutón, María Jesús (MDPI, 2010)
      The condensation of 3-methoxy or 3-ethoxy-2-hydroxybenzaldehyde and 1,2 diamine -2-methylpropane, to yield at the dianionic hexadentate Schiff base ligands H2 Ln (H2 L1 , H2 L2 respectively). The ligands have been characterised ...
    • Double imidazolidine condensation in a polynucleating Schiff base 

      Fondo Busto, María Matilde; García Deibe, Ana María; Ocampo Prado, Noelia; Sanmartín Matalobos, Jesús (MDPI, 2010)
      Condensation of pentaethylenehexamine and 3-bromo-5-chlorosalicylaldehyde yielded the bisimidazolidine Schiff base ligand 5,6\'-(1E,1\'E)-(2,2\'-(3,3\'-(ethane-1,2- diyl)bis(2-(3-bromo-5-chloro-2-hydroxyphenyl)imidazolid ...
    • Crystal structure of (n-n'-bis(3-ethoxysalicylidene)-1,2-diaminopropane 

      Vázquez Fernández, María de los Ángeles; Fernández García, María Isabel; Fernández Fernández, Beatriz; González Noya, Ana María; Maneiro Maneiro, Marcelino; Rodríguez Doutón, María Jesús (MDPI, 2009)
      Three hexadentate Schiff base ligands were obtained by condensation of 3-ethoxy-2-hydroxybenzaldehyde and different diamines (1,2-diaminoethane, 1,2-diaminopropane, 1,2-diamino-2-metylpropane) to yield H2Ln (H2L1, H2L2 and ...
    • The crystal structure of a compartmental heptadentate ligand 

      Fondo Busto, María Matilde; Ocampo Prado, Noelia; García Deibe, Ana María; Sanmartín Matalobos, Jesús (MDPI, 2009)
      2-(2-hydroxyphenyl)-1,3-bis[4-(2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine (H3L) was obtained with high purity by Schiff's condensation between 5-bromosalicyaldehyde and triethylenetetramine. Its recrystallisation ...





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