Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves
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Título: | Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves |
Autor/a: | Seijas Vázquez, Julio Antonio Vázquez Tato, María del Pilar Crecente Campo, José |
Centro/Departamento: | Universidade de Santiago de Compostela. Departamento de Química Orgánica |
Data: | 2006 |
Editor: | MDPI |
Cita bibliográfica: | Seijas, J.A.; Vázquez-Tato, M.P.; Crecente-Campo, J. Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves, in Proceedings of the 10th International Electronic Conference on Synthetic Organic Chemistry, 1–30 November 2006, MDPI: Basel, Switzerland, doi:10.3390/ecsoc-10-01442 |
Serie: | Electronic Conference on Synthetic Organic Chemistry;10 |
Resumo: | Microwave assisted organic synthesis (MAOS) of N,N-diisopropyl enol carbamate of acetophenone is achieved in good yield when acetophenone, N,N-diisopropylcarbamoyl chloride and Hüning's base, DABCO or TMEDA were irradiated with microwaves. It is remarkable that reaction times are reduced from six days with conventional heating, to twenty minutes |
Descrición: | The 10th International Electronic Conference on Synthetic Organic Chemistry session Symposium on Microwave Assisted Synthesis |
Versión do editor: | https://doi.org/10.3390/ecsoc-10-01442 |
URI: | http://hdl.handle.net/10347/26821 |
DOI: | 10.3390/ecsoc-10-01442 |
ISBN: | 3-906980-18-9 |
Dereitos: | ©2007 by MDPI, Basel, Switzerland. Open Access |