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dc.contributor.authorPérez Mayán, Leticia
dc.contributor.authorRamil Criado, María
dc.contributor.authorCela Torrijos, Rafael
dc.contributor.authorRodríguez Pereiro, Isaac
dc.date.accessioned2021-09-23T12:19:11Z
dc.date.available2021-09-23T12:19:11Z
dc.date.issued2021
dc.identifier.citationJournal of Food Composition and Analysis 104 (2021) 104184. https://doi.org/10.1016/j.jfca.2021.104184
dc.identifier.issn0889-1575
dc.identifier.urihttp://hdl.handle.net/10347/26945
dc.description.abstractLiquid chromatography tandem mass spectrometry (LC–MS/MS) has been combined with different sample preparation strategies to determine potential pesticide residues existing in wine. Herein, we propose the on-line coupling between solid-phase extraction (SPE), based on a reversed-phase polystyrene-divinyl benzene (PS-DVB) sorbent, and LC–MS/MS for the automated monitoring of a selection of 48 pesticides (37 fungicides and 11 insecticides) in this beverage. Parameters affecting the sensitivity, selectivity, accuracy and robustness of the method are evaluated as function of sample volume, clean-up conditions, and number of extraction-desorption cycles performed with the same SPE cartridge
dc.description.sponsorshipL.P.M thanks a FPU grant to the Spanish Ministry of Science. This study was supported by Spanish Government and Xunta de Galicia through grants PGC2018-094613-B-I00 and ED431C 2021/06, both co- funded by the EU FEDER program. We acknowledge Agilent for providing access to the LC-ESI-MS/MS instrumentation employed in this study
dc.language.isoeng
dc.publisherElsevier
dc.relationinfo:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/PGC2018-094613-B-I00/ES/ESPECTROMETRIA DE MASAS COMBINADA CON SISTEMAS DE INTRODUCCION DE MUESTRA RESUELTOS EN EL TIEMPO Y DIRECTOS. APLICACIONES ANALITICAS CUANTITATIVAS Y DE SCREENING
dc.rights© 2021 The Authors. Published by Elsevier Inc. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
dc.rightsAttribution-NonCommercial-NoDerivatives 4.0 Internacional
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/4.0/
dc.subjectPesticides
dc.subjectWine
dc.subjectOn-line SPE
dc.subjectLiquid chromatography
dc.subjectTandem mass spectrometry
dc.titleDetermination of pesticide residues in wine by solid-phase extraction on-line combined with liquid chromatography tandem mass spectrometry
dc.typeinfo:eu-repo/semantics/article
dc.identifier.DOI10.1016/j.jfca.2021.104184
dc.relation.publisherversionhttps://doi.org/10.1016/j.jfca.2021.104184
dc.type.versioninfo:eu-repo/semantics/publishedVersion
dc.rights.accessrightsinfo:eu-repo/semantics/openAccess
dc.contributor.affiliationUniversidade de Santiago de Compostela. Departamento de Química Analítica, Nutrición e Bromatoloxía
dc.description.peerreviewedSI


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© 2021 The Authors. Published by Elsevier Inc. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
Except where otherwise noted, this item's license is described as  © 2021 The Authors. Published by Elsevier Inc. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)





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