| dc.contributor.author | Pérez Mayán, Leticia |
| dc.contributor.author | Ramil Criado, María |
| dc.contributor.author | Cela Torrijos, Rafael |
| dc.contributor.author | Rodríguez Pereiro, Isaac |
| dc.date.accessioned | 2021-09-23T12:19:11Z |
| dc.date.available | 2021-09-23T12:19:11Z |
| dc.date.issued | 2021 |
| dc.identifier.citation | Journal of Food Composition and Analysis 104 (2021) 104184. https://doi.org/10.1016/j.jfca.2021.104184 |
| dc.identifier.issn | 0889-1575 |
| dc.identifier.uri | http://hdl.handle.net/10347/26945 |
| dc.description.abstract | Liquid chromatography tandem mass spectrometry (LC–MS/MS) has been combined with different sample preparation strategies to determine potential pesticide residues existing in wine. Herein, we propose the on-line coupling between solid-phase extraction (SPE), based on a reversed-phase polystyrene-divinyl benzene (PS-DVB) sorbent, and LC–MS/MS for the automated monitoring of a selection of 48 pesticides (37 fungicides and 11 insecticides) in this beverage. Parameters affecting the sensitivity, selectivity, accuracy and robustness of the method are evaluated as function of sample volume, clean-up conditions, and number of extraction-desorption cycles performed with the same SPE cartridge |
| dc.description.sponsorship | L.P.M thanks a FPU grant to the Spanish Ministry of Science. This study was supported by Spanish Government and Xunta de Galicia through grants PGC2018-094613-B-I00 and ED431C 2021/06, both co- funded by the EU FEDER program. We acknowledge Agilent for providing access to the LC-ESI-MS/MS instrumentation employed in this study |
| dc.language.iso | eng |
| dc.publisher | Elsevier |
| dc.relation | info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/PGC2018-094613-B-I00/ES/ESPECTROMETRIA DE MASAS COMBINADA CON SISTEMAS DE INTRODUCCION DE MUESTRA RESUELTOS EN EL TIEMPO Y DIRECTOS. APLICACIONES ANALITICAS CUANTITATIVAS Y DE SCREENING |
| dc.rights | © 2021 The Authors. Published by Elsevier Inc. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/) |
| dc.rights | Attribution-NonCommercial-NoDerivatives 4.0 Internacional |
| dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0/ |
| dc.subject | Pesticides |
| dc.subject | Wine |
| dc.subject | On-line SPE |
| dc.subject | Liquid chromatography |
| dc.subject | Tandem mass spectrometry |
| dc.title | Determination of pesticide residues in wine by solid-phase extraction on-line combined with liquid chromatography tandem mass spectrometry |
| dc.type | info:eu-repo/semantics/article |
| dc.identifier.DOI | 10.1016/j.jfca.2021.104184 |
| dc.relation.publisherversion | https://doi.org/10.1016/j.jfca.2021.104184 |
| dc.type.version | info:eu-repo/semantics/publishedVersion |
| dc.rights.accessrights | info:eu-repo/semantics/openAccess |
| dc.contributor.affiliation | Universidade de Santiago de Compostela. Departamento de Química Analítica, Nutrición e Bromatoloxía |
| dc.description.peerreviewed | SI |
